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systems is to measure the time for a dispersion to separate. The tested system is thoroughly agitated to form either a water-in-oil (w/o) or oil-in-water (o/w) dispersion, depending on the system under investigation. Following 3 to 5 min of vigorous agitation or shaking, the system is allowed to settle and the time to form two distinct layers is noted. Complete separation may not occur, but two distinct layers ought to be visible. Guidelines for scale-up, based on separation time, are given in Table 12-3. When applying this method, be aware that density differences affect both settling time and the forces acting on the drops that cause lm drainage. If coalescence appears to be severe and undesirable, reverse the phases if possible and repeat the test. Finally, compare the times for coalescence to see which phase should be dispersed. A more quantitative method is to use a baf ed stirred vessel containing a light transition probe similar to the one described by Rodger et al. (1956). Record the probe output at moderately high levels of agitation. After a constant baseline is established, reduce the agitation to just maintain full suspension and observe changes in the recorded output. The probe can be calibrated to read interfacial area. The slope at the time just after speed transition is proportional to the rate of coalescence under dynamic as opposed to static conditions. This method is insensitive to effects of density difference and is described by Howarth (1967). If the interfacial area appears to remain constant after decreasing the agitation, the system can be considered to be noncoalescing. If not, the steepness of the asp.net data matrix reader ASP.NET Data Matrix Barcode Reading Decoder Library | Free VB ...
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